Radioactive sample experiment: Radioactive samples can only be solid or liquid, packaged according to radiation protection requirements. Before the experiment, detailed reporting and relevant procedures need to be completed.

Non radioactive sample experiment: According to different experimental methods, the specific details are as follows:

Diffraction related: Mainly solid and powder, powder can be compressed or encapsulated in capillaries.

Spectroscopy related equipments: Solid, powder, solution, thin film, powder tablet (preferred) or coated with tape. The sample size is generally greater than 3 × 3 mm².

Microbeam related equipments: Solid, thin film.