Beamline Introduction
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The soft X-ray spectromicroscopy beamline is one of the first seven beamlines built in the first phase project of the Shanghai Synchrotron Radiation Facility (SSRF). It adopts an elliptically polarized undulator light source with high photon flux and good spatial coherence. Its photon energy is selected between 200eV and 2000eV, and this energy range covers the absorption edges of most of the important elements in the fields of biology, environment (soil, minerals), polymers, nanomaterials, etc., such as the K absorption edges of C, N, O, F, Na, and Mg, the L edges of Cl, K, Ca, Fe, Cu, and Zn in living cells. The scanning transmission X-ray microscopy (STXM) of this beamline combines the high spatial resolution (better than 30 nm, and up to 10 nm in combination with the CDI method) with the high chemical state resolution capability of near-edge absorption fine structure spectroscopy (NEXAFS), which enables the study of the properties of a wide range of physical states, such as solids, liquids, and soft matter, at the nanoscale.
Scientific Scope
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► Materials Science (Effects of doping elements on materials properties);

► Biomedicine (sub-micron spatial and chemical analysis of cells, bacteria, tissues, etc.);

► Environmental science (soil, fungus-harmful metal interactions and spatial distribution, etc.);

► Design of nanodevices;

► Magnetic imaging and magnetic properties research, etc.

Beamline Layout
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Specifications
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 Photon energy range  200 - 2000 eV
 Energy resolution (E/E)  > 17000 @244eV
 4200 @867eV
 Minimum spot size  30 nm
 Photon flux  1.5×108phs/s@410eV
Endstations
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1)STXM platform
Detectors: Photomultiplyer tube (PMT), PhotoDiode(PD), Optical microscope, X-ray CMOS camera, Silicon Drift Detector (SDD)
Sample stages: 3D piezo ceramic scanner, 2D high precision stepping scanner, High precision rotation stage
Focusing system: Fresnel zone-plate, Order-selecting aperture
2)XAS platform
Detectors: TEY measurement system, Silicon drift detector, XEOL fiber probe
Sample stage: 4D high precision moving stage
In-situ equipments: VTI cryo pole, Compactor, Thermocouple heating system, Electromagnet
Data Acquisition and Analysis
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1)Imaging Methods
► Scanning transmission imaging -- 30 nm spatial resolution
► Dual energy contrast imaging -- 2D distribution and content of specific elements within a substance
► Energy stack imaging -- Spatial distribution of chemical states of elements
► Ptychography -- lensless imaging with better than 10nm resolution
► Nano-CT -- Nanoscale 3D imaging of samples and 3D distribution of elements
2)Spectroscopic Methods
► Total electron yield (TEY) spectroscopy -- Near-edge absorption spectra of elements, focusing on sample surface elements.
► Partial fluorescence yield (PFY) spectroscopy -- Near-edge absorption spectra of elements, focusing on low-content elements and bulk phase information
► Magnetic circular dichroism/linear dichroism (XMCD/XLD) -- Measurement of magnetic properties of samples
► Soft X-ray excited optical luminescence (XEOL) spectroscopy -- Combined with TEY for studying the luminescence mechanism of materials
3)Operating instructions
BL08U1A Users Manual.pdf (Download link)
STXM dimming brief tutorial.ppsx (Download link)
Experimental procedures for Soft X-ray spectromicroscopy.pptx (Download link)
4)Data processing
Software runtime environment installation file: IDL.zip (Download link)
Dual energy image processing software: Dual-Energy-Element-Distribution.sav (Download link)
Stack image processing software: stack_analysis.zip (Download link)
Documentation of data processing instructions: Spectromicroscopic data analysis.pptx (Download link)
English instructions on stack image processing: pca_gui_man.pdf (Download link)